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关注：1
2013-05-23 12:21
求翻译：The observed reaction mixture was stirred with heating at 60–70 ◦C in a water bath for 1.5 h. After this time of period the solvent was removed under reduced pressure and to the obtained residue, 1 equivalent of the corresponding 2-chloro-N-alkylacetamide dissolved in DMF was added.是什么意思？ 待解决
 悬赏分：1
- 离问题结束还有
The observed reaction mixture was stirred with heating at 60–70 ◦C in a water bath for 1.5 h. After this time of period the solvent was removed under reduced pressure and to the obtained residue, 1 equivalent of the corresponding 2-chloro-N-alkylacetamide dissolved in DMF was added.
问题补充： |
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2013-05-23 12:21:38
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2013-05-23 12:23:18
观察到的反应混合物的搅拌加热 60 — 70 ◦C 在水浴为 1.5 h 。 在这时间之后的期间内的溶剂是被减少的压力和获得的残留物、 1 相当于对应的 2 - 氯 - N - alkylacetamide 溶解在 DMF 被添加。
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2013-05-23 12:24:58
被观察的反应混合物在热水锅搅动了以加热在60-70 ◦C为1.5 h。 在期间以后的这时期溶剂在减压下被去除了，并且对获得的残滓， 1个等值对应的2chloroN ALKYLACETAMIDE溶化在DMF增加了。
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2013-05-23 12:26:38
将观察到的反应混合物在 60-70 摄氏度为 1.5 h 的水浴中加热搅拌。溶剂中移除了下这段时间减少压力和到所得的残留物，1 个相当于相应的 2-氯-N-alkylacetamide 中溶解后 DMF 又加上。
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2013-05-23 12:28:18
正在翻译，请等待...
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