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关注:1 2013-05-23 12:21

求翻译:To do the reaction, a 1000 ml round bottom flask is filled with 150 grams of ephedrine hydrochloride (or PPA-HCl). The use of the sulfate salt is unacceptable because HI reduces the sulfate ion, so this interferes with the reaction. Also added to the flask are 40 grams of red phosphorus and 340 ml of 47% hydroiodic acid. This same acid and red phosphorus mixture can be prepared from adding 150 grams of iodine crystals to 150 grams of red phosphorus in 300 ml of water. This should produce the strong hydroiodic acid solution needed. Exactly how strong the acid needs to be, I can't say . I can tell you that experiments have shown that one molar HI is ineffective at reducing ephedrine to meth. The 47% acid mentioned above is a little over 3.5 molar. I would think that so long as one is over 3 molar acid, the reaction will work.是什么意思?

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To do the reaction, a 1000 ml round bottom flask is filled with 150 grams of ephedrine hydrochloride (or PPA-HCl). The use of the sulfate salt is unacceptable because HI reduces the sulfate ion, so this interferes with the reaction. Also added to the flask are 40 grams of red phosphorus and 340 ml of 47% hydroiodic acid. This same acid and red phosphorus mixture can be prepared from adding 150 grams of iodine crystals to 150 grams of red phosphorus in 300 ml of water. This should produce the strong hydroiodic acid solution needed. Exactly how strong the acid needs to be, I can't say . I can tell you that experiments have shown that one molar HI is ineffective at reducing ephedrine to meth. The 47% acid mentioned above is a little over 3.5 molar. I would think that so long as one is over 3 molar acid, the reaction will work.
问题补充:

  • 匿名
2013-05-23 12:26:38
若要做反应,圆底烧瓶的 1000 毫升充满麻黄碱盐酸盐 (或苯丙醇胺盐酸) 150 克。硫酸盐的使用是不能接受的因为喜降低硫酸根离子,所以这会干扰反应。赤磷 40 克和 47%碘酸 340 毫升的需要,还会添加到瓶。这同样的酸和红色的磷混合物可以准备从碘晶体 150 克加入赤磷 300 毫升的水 150 克。这应产生所需的强大 hydroiodic 酸溶液。究竟如何强酸的需要,我不能说。我可以告诉你实验表明一个摩尔喜在减少甲基麻黄碱无效。上文所述的 47%酸是有点超过 3.5 磨牙。我认为,只要其中一个是超过 3 摩尔酸,将工作反应。
 
 
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